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Synthesis, characterization and electrochemical investigations of heterocyclic-selenocarboxylate iron complexes

Abstract : Selenocarboxylato complexes of iron containing heterocyclic group of the general formula CpFe(CO)2SeCO-het [het = 2-C4H3S (1), 2-C4H3O (2), -CH2-2-C4H3S (3)] were prepared from the reaction of iron selenide, (μ-Se)[FeCp(CO)2]2 and the corresponding heterocyclic acid chlorides. These complexes have been characterized by elemental analysis, UV-Vis, IR and 1H NMR spectroscopic techniques. The X-ray structure of 1 is determined and its electrochemical behavior has been described in details applying cyclic voltammetry. © 2016 Elsevier B.V.
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https://hal.univ-brest.fr/hal-01770460
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Submitted on : Thursday, April 19, 2018 - 9:21:55 AM
Last modification on : Tuesday, December 10, 2019 - 5:30:08 PM

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M. El-Khateeb, H. Abul-Futouh, H. Görls, W. Weigand, Laith.R Almazahreh. Synthesis, characterization and electrochemical investigations of heterocyclic-selenocarboxylate iron complexes. Inorganica Chimica Acta, Elsevier, 2016, 449, pp.14-19. ⟨10.1016/j.ica.2016.04.033⟩. ⟨hal-01770460⟩

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