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Synthesis of O,O -Diethyl Arylthiophosphonate from O -Aryl- O , O -diethylthiophosphate

Thierno Dieng 1 Aurore Fraix 1 Jean-Yves Salaün 1 Isabelle Dez 2 Robertus Klein Gebbink 3 Gerard van Koten 3 Paul-Alain Jaffres 1
1 CEMCA - Chimie, Electrochimie Moléculaires et Chimie Analytique
2 LCMT - Laboratoire de chimie moléculaire et thioorganique
3 HU - University of Applied Sciences [Utrecht]
Abstract : The synthesis of O,O-diethyl 2-hydroxyarylthiophosphonate is reported by using a [1,3]-rearrangement. This method is achieved in high yield from ortho-bromophenols derivatives by a two-step process
Keywords : phosphorylation metallation phenols rearrangement
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Journal articles
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https://hal.univ-brest.fr/hal-01580497
Contributor : Nicolas Renard <>
Submitted on : Friday, September 1, 2017 - 4:01:44 PM
Last modification on : Thursday, July 2, 2020 - 3:21:25 AM

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UNIV-BREST | CEMCA-BREST | CNRS | INC-CNRS | COMUE-NORMANDIE | ENSICAEN | UNICAEN | LCMT | IBSAM | UNILEHAVRE | INSA-ROUEN | UNIROUEN | INSA-GROUPE

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Thierno Dieng, Aurore Fraix, Jean-Yves Salaün, Isabelle Dez, Robertus Klein Gebbink, et al.. Synthesis of O,O -Diethyl Arylthiophosphonate from O -Aryl- O , O -diethylthiophosphate. SYNLETT, Georg Thieme Verlag, 2008, 2008 (20), pp.3121 - 3124. ⟨10.1055/s-0028-1087362⟩. ⟨hal-01580497⟩

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