Elaboration and characterization of novel polyamide-12-layered titanoniobates nanocomposites

Sophie Chausson 1 Richard Retoux 1 Jean-Michel Rueff 1 Loïc Le Pluart 2 Pierre-Jean Madec 2 Paul-Alain Jaffres 3
1 CRISMAT - Laboratoire de cristallographie et sciences des matériaux
2 LCMT - Laboratoire de chimie moléculaire et thioorganique
3 CEMCA - Chimie, Electrochimie Moléculaires et Chimie Analytique
Abstract : This article describes the synthesis and the characterization of a polyamide-12 filled with a nanostructured organic/inorganic titanoniobate hybrid material. The pristine oxide KTiNbO5 has been successfully organomodified by N-alkyl amines via an acido-basic reaction after a cationic exchange step as shown by x-ray diffraction. Transmission electron microscope study and scanning transmission electron microscope observations have been used to describe the change of morphology of the nanofillers before and after processing; the micronic aggregates were changed into single sheets and dispersed in the polymer. Thermomechanical properties of the composites have been determined, and their analyses with structure-properties models are consistent with the exfoliation of the organomodified titanoniobates.
Type de document :
Article dans une revue
Journal of Materials Research, Cambridge University Press (CUP), 2009, 24 (11), pp.3358 - 3371. 〈10.1557/jmr.2009.0410〉
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http://hal.univ-brest.fr/hal-01580240
Contributeur : Nicolas Renard <>
Soumis le : vendredi 1 septembre 2017 - 11:05:40
Dernière modification le : jeudi 19 juillet 2018 - 12:04:02

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UNIV-BREST | CEMCA-BREST | INC-CNRS | COMUE-NORMANDIE | ENSICAEN | LCMT

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Sophie Chausson, Richard Retoux, Jean-Michel Rueff, Loïc Le Pluart, Pierre-Jean Madec, et al.. Elaboration and characterization of novel polyamide-12-layered titanoniobates nanocomposites. Journal of Materials Research, Cambridge University Press (CUP), 2009, 24 (11), pp.3358 - 3371. 〈10.1557/jmr.2009.0410〉. 〈hal-01580240〉

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