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R. I. Prout and K. , Job plot for the reaction of 1 with Na[BAr F 4 ] in CD 2 Cl 2 (bottom left) and solid-state structure of EE-2 (below bottom right; thermal ellipsoids at 50% probability, minor disordered component omitted for clarity). 6 Reagents and conditions: (i) 0.5 equiv. Na[BAr F 4 ], CH 2 Cl 2 , 293 K; (ii) Grubbs I h; (iii) HCl then Et 3 N (51% yield of 2 over 3 steps); (iv) Wilkinson's catalyst, 002 M, CH 2 Cl 2 , 293 K toluene, 323 K, 20 h (quantitative yield). using CRYSTALS (Betteridge, P. W.; Carruthers

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